MOUDI-II™ & NanoMOUDI-II™ Overview
The Moudi consists of two main parts: the cascade impactor itself and its associated housing, with hinged door access. The combined unit measures 210 x 210 x 641 mm and weighs approximately 14 kg.
The non-rotating version of the NanoMoudi (Model
125A) operates as a conventional impactor and is supplied without the housing.
In the rotating versions, Models
120 and
125B, the nozzle and impaction plates rotate at 1 rpm relative to each other, to form a near-uniform particle deposit on each substrate.
This has the effect of increasing the deposited particle mass by a factor of up to 1000, thus more particle mass can be collected without the risk of overloading.
The
rotational motion is generated by individual stepper motors which drive the impaction plates at each stage (see schematic). Power for the stepper motors is controlled via electronics contained with the housing of the impactor, with power being distributed to each motor by miniature flat-ribbon cables from stage to stage.
The housing also contains electronics for precisely controlling the volumetric flow rate. These provide a readout of the cabinet temperature and also the six absolute pressure readings from the transducers used to monitor pressure between the more critical micro-orifice stages of the impactor.
The flow stability data derived from these measurements provides a quick and easy means of identifying any problems emanating from
leaks or blocked nozzles within the system.
If, for example, one or more of the absolute pressures on the stages begins to drop while the flow remains constant, it indicates that the nozzles in these stages are becoming dirty and should be cleaned. The micro-orifice nozzles used in the final stages are quite small and can become partially occluded due to particle deposition by impaction or diffusion (Brownian and turbulent). When this occurs, the pressure drop across the nozzle plates will rise.
The
Moudi Model 120 has a flow rate of
30 L/min and cut sizes from 18 microns at the inlet to 56 nanometres at the lowest stage. The standard configuration is
ten stages (eleven including the inlet) with cut sizes at 18, 10, 5.6, 3.2, 1.8, 1.0, 0.56, 0.32, 0.18, 0.10 and 0.056 microns plus final filter.
The NanoMoudi Model 125 has a sampling rate of
10 L/min and cut sizes spanning the range from 10 microns to 10 nanometres. The standard configuration is
thirteen stages with cut sizes at 10, 5.6, 3.2, 1.8, 1.0, 0.56, 0.32, 0.18, 0.10, 0.056, 0.032, 0.018 and 0.010 microns plus final filter.
A suitable vacuum pump is required to generate the desired flow rate.
The
impaction plates can be prepared in the laboratory and inserted into the impactor at the time of use. Covers are provided for the plates to keep them clean during transit. The impactors were designed and calibrated based on the use of a 25 nm thick
substrate having a diameter of 47 mm. Aluminium foil, teflon film or thin membrane filters are also suitable.
In some cases, it may be necessary to apply a sticky surface to the substrates to reduce particle bounce. This is normally the case if foils are used and the sampled particles are dry.
Special
coating masks (with a 37 mm diameter hole punched in the centre) used in conjunction with a
silicone spray are available as options and are ideal for this purpose.
If the mass size distribution is to be determined from the impactor, the substrates must be weighed before and after a run. It is important that the weight of the sticky material applied to the substrate be stable. It is essential therefore to ensure that all the solvent be evaporated completely before use.
In the case of the rotating versions, overall control of the impactor is assumed by a programmable VGA display/controller located on the front of the housing and accessed by means of a membrane keypad.
The unit can be operated in two modes: manual or timed operation. Under manual operation, the vacuum pump switches on, all of the impaction plates start to rotate and the sensor outputs begin to transmit data to the screen immediately the 'start' button is pressed. Operation will continue and data collected at 1 minute intervals until terminated by the 'stop' button.
Under timed operation, the start and end of the run is predetermined by the operator. Sampling times can be adjusted between 5 minutes and 7 days with appropriate data logging intervals of between 1 and 15 minutes. The sampling interval should be selected such as to provide sufficient mass for subsequent gravimetric or chemical analysis. Check the inlet flow rate using a suitable flow meter prior to the start of the test.
Additional controls serve to download and erase the environmental and pressure related data from the memory.
Applications
- Environmental Monitoring
- Sampling of atmospheric aerosols
- Nanoparticle research
- Chemical composition of Ultra-fine particles
- Industrial Hygiene and Occupational Health Studies
- Process Aerosol Analysis
- Biological Contamination: Hospital, Civil & Military Defence
- Size-fractionated gravimetric or chemical analysis
- Diesel and gasoline emission analysis and monitoring
- Pharmaceutical inhalation research